r about an hour.
Next 100 ml of methylenedioxyphenylacetone is added along with 40
grams NHUCl, 500 ml methyl alcohol saturated with ammonia gas,
and 50 ml NHjOH. The bottle is then set up as seen in Figure 17 in
Secrets of Methamphetamine Manufacture, Third Edition. The
hydrogenation is done as described in that section.
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When the reduction is over, the contents of the flask are filtered to
remove the platinum metal for reuse. Some crystals of NH4C1 are also
filtered out; they are rinsed down with some water to remove them.
Next the filtered batch is poured into a 1000 ml round-bottom
flask, a few boiling chips are added, and the glassware is set up for
refluxing. Plastic tubing is attached to the top of the condenser and
led outside. The mixture is boiled under reflux for one hour to force
out the excess ammonia.
Next, the solution is allowed to cool, and made acid to congo red
(about pH 3) with hydrochloric acid. Now the glassware is set up as
shown in Figure 3 of Secrets of Methamphetamine Manufacture,
Third Edition, and the solution is evaporated to about one-half its
original volume under vacuum. A fair amount of crystalline material
forms during the acidification and vacuum evaporation.
Next, 400 ml of water is added to the solution, and then it is
extracted with about 100 ml of toluene. The toluene layer is thrown
away because it contains garbage. The batch is now made strongly
basic by adding lye water to it. It should be remembered here that it is
very important to shake the batch well once it has been basified, to
make sure that the MDA hydrochloride gets neutralized. Finally, the
MDA is extracted out with a few hundred ml of toluene, and distilled
under vacuum. The boiling point is about 160fi C under aspirator
vacuum. The yield is about 50 ml.
Another very good choice of a method for converting
methylenedioxyphenylacetone to MDA is the Leuckardt reaction. In
this case formamide is used instead of N-methyl formamide. When
used with phenylacetone to make amphetamine, only the very highgrade
99% material will work. In the case of methylenedioxyphenylacetone,
however, the much more commonly available 98%
formamide works just fine. See Chem. Abstracts from 1952, column
11246, and Austrian patent 174,057. In this variation, 40 ml of
methylenedioxyphenylacetone is mixed with 100 ml of freshly
vacuum-distilled formamide, 2 ml glacial acetic acid, and 20 ml
water. This mixture is heated up to about 130° C, at which point
bubbling should begin, then the temperature is slowly raised to keep
72 Studies On The Production OfTMA-2
the bubbling going, as described in Chapter 5 of Secrets of
Methamphetamine Manufacture, Third Edition, until a temperature of
ISO° C is reached. This should take at least 5 hours. The yield is 70%.
Processing is then done just as in the case of meth. The
formamide is destroyed by boiling with lye solution. In this case, the
ammonia gas produ
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These approaches may be less useful in individuals with normal testosterone levels, as the body's regulatory mechanisms tend to respond to an excess of testosterone by shutting down its own testosterone production, (" SHBG ")
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